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With an exception to human error during the experiment & making calculations, the outcome is the same. Another difference in products was caused by the impurities in the reagents that were not completely filtered out during the experiment. By looking at the NMR spectra of the Amide and Ether route, you can see unknown peaks of impurities that do not correspond to the product...
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Acetophenetidin can be formed through two methods, Williamson ether synthesis and amide synthesis. By working in groups of two we were able to complete both methods of synthesis routes. The end result should be the synthesis of a similar product, by verification between the two individuals.
Experiment and Observations
Amide Synthesis of Acetophenetidin
The Synthesis reaction began by removing the colored impurities from the p-phenetidine, accomplished by mixing with HCl and heating...
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