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Science
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3 / 701 |
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The rise in melting point range in this experiment is most likely due to improper time allotted for the gravity filtration to complete. Since too short of time was most likely given to this portion of the experiment, the pure compound left behind (which we used in our melting point determination) may not have been completely dry...
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If the solid was not completely dry, the melting point of our unknown solid would have decreased. This is shown accurately by the regular melting point range of salicylic acid being 158 ? C - 160 ? C, and the discovered melting point range being slightly lower at 147 ? C -149 ? C. Since the final melting point range was 154 ? C - 156 ? C, it makes sense that salicylic acid would be the correct identity of the unknown, because this range falls right in the middle...
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