Buy custom Preparation of 2-acetylcyclohexanone
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Science
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| Number of pages / Number of words: |
6 / 1664 |
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Enamines are very easily alkylated due to them being very nucleophillic1.
The first step entails the reaction of pyrrolidine and cyclohexanone with p-Toluenesulfonic acid to form a toluene solution of the enamine as shown below.
Step 1: Reaction of pyrrolidine and cyclohexanone with p-Toluenesulfonic acid to form a toluene solution of the enamine
The second step involves the reaction of the toluene solution of the enamine with acetic anhydride to form 1-pyrrolidino-1-cyclohexene, which is the intermediate of the reaction...
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This intermediate is not seen as it cannot be isolated due to it being very unstable.
Step 2: Reaction of the enamine with the acetic anhydride to form 1-pyrrolidinocyclohexene (the intermediate)
The third and final step is the reaction of the intermediate(1-pyrrolidino-1-cyclohexene) with water in order to form final product 2-acetylcyclohexanone...
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