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Mix these thoroughly and then add 0.63 g of silica gel. Stopper the flask and mix until the silica gel is evenly and completely covered with reactants.
Cover the flask with a watch glass and microwave on high for 5 times 2 minutes (total of 10 minutes) giving a quick swirl between intervals.
Once the reaction has reached room temperature, add about 15 mL of ethyl acetate...
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Filter to remove the silica gel. Spot your product solution on a TLC plate and develop with a 7:1 hexanes/ethyl acetate eluent. Your product should be a purple spot. Report the Rf of the product and any indication by TLC of other materials/impurities.
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