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| Topic: |
Science
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| Number of pages / Number of words: |
5 / 1146 |
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The entire apparatus was put in a heated sand bath. The apparatus was closely monitored during boiling so that the distillation rate was no faster than 2 drops per minute.
After a couple milliliters of sample were collected, the sample was poured onto a watch glass. The sample was then lit by a match to test how much of it burned...
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Any remaining sample was washed down the drain.
For fractional distillation, I added 4 mL of a 10-20% ethanol-water mixture to a 5-mL short-necked flask. I joined the flask to a distilling column that was packed with thickly with some steel wool. This was then joined to a distilling head with a thermometer through a rubber connector...
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