Buy custom Bromination of benzene: synthesis and purification of bromobenze
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Science
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3 / 616 |
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Place the filtered liquid in a round bottom flask.
Set up a distillation apparatus. Place the bromobenzene is a round bottom flask and distill into a clean flask. Collect the distillate only from between 150-160OC. Re-distil this liquid to obtain a more pure solution of bromobenzene. The liquid collected from this distillation should be between 155-156OC...
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The liquid collected from this distillation should be between 155-156OC. It should be colorless and have a slightly "agreeable odor." This will be considered the "pure" bromobenzene and the reaction yield should be 80%.
Purity tests:
Test 1:
Determine the boiling point of the liquid by measuring a boiling point range during the distillation...
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