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If solid does not appear, reheat flask in hot water bath and cool again.
Set up vacuum filtration apparatus. Insert filter paper into funnel and turn on water aspirator. Decant the liquid onto the filter paper, being very careful to keep the transfer of any solid to a minimum. Add 15mL of cold water to flask, swirl, and chill again...
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Add 15mL of cold water to flask, swirl, and chill again. Pour liquid and crystals onto filter paper. Repeat process until transfer of the crystals is complete. Wash crystals with 10mL of water, and utilize the vacuum to dry the crystals as best as possible. Determine and record the mass of the crude aspirin...
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