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An engineering principal states that the total volume of a tank must be replaced three times to be 95% confident that the outlet stream is representative of an upstream change. For the tank that we sample, the volume is exchanged every 15 minutes. Therefore, we wait an hour before taking a sample after making a process change, so that we are over 95% certain that the change we made is reflected in the sample taken...
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It has been determined that four samples are required for at least a 95% confidence that the difference between groups of samples was not caused by variability in our analytical tests. To maintain at least a 95% confidence in our results, we take a sample every hour for four hours before and after our change...
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