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Buy custom Preparation of 2-acetylcyclohexanone

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Topic: Science
Number of pages / Number of words: 6 / 1664
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Enamines are very easily alkylated due to them being very nucleophillic1.

The first step entails the reaction of pyrrolidine and cyclohexanone with p-Toluenesulfonic acid to form a toluene solution of the enamine as shown below.

Step 1: Reaction of pyrrolidine and cyclohexanone with p-Toluenesulfonic acid to form a toluene solution of the enamine

The second step involves the reaction of the toluene solution of the enamine with acetic anhydride to form 1-pyrrolidino-1-cyclohexene, which is the intermediate of the reaction...


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This intermediate is not seen as it cannot be isolated due to it being very unstable.

Step 2: Reaction of the enamine with the acetic anhydride to form 1-pyrrolidinocyclohexene (the intermediate)

The third and final step is the reaction of the intermediate(1-pyrrolidino-1-cyclohexene) with water in order to form final product 2-acetylcyclohexanone...


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