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| Topic: |
Science
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| Number of pages / Number of words: |
7 / 1695 |
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See calculations section for explanation.
Overall Reaction: C8H10O2 + 2C4H10O ?? C16H26O2 + 2H2O
1,4-di-t-butyl-2,5-dimethoxybenzene H2SO4 1, 4-dimethoxybenzene OCH3 OCH3 + OH CH3 CH3 CH3 Tert-butyl alcohol OCH3 OCH3 H2O +
Mechanism:
H H H O SO3H Sulfuric Acid OH CH3 CH3 CH3 O CH3 CH3 CH3 + + CH3 CH3 CH3 C
Friedel-Crafts Alkylation Reaction
Mechanism (con't) + CH3 CH3 CH3 C OCH3 OCH3 + OCH3 OCH3 H + OCH3 OCH3 H + OCH3 OCH3 H -OSO3H OCH3 OCH3 + H OCH3 OCH3 + + CH3 CH3 CH3 C OCH3 OCH3 -OSO3H H OCH3 OCH3 + H OCH3 OCH3 OCH3 OCH3 H2SO4 + 1,4-di-t-butyl-2,5-dimethoxybenzene
Procedure:
Dissolve 120 mg 1,4-dimethoxybenzene in a 10 x 100 mm reaction tube with 0...
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Add to it 0.2 mL t-butyl alcohol and heat gently until the mixture is in solution. Once it's in solution, cool the mixture in ice. Then, add 0.4 mL concentrated H2SO4 (18 M) to the tube dropwise with a Pasteur pipet. After each drop is added, mix the solution thoroughly with a glass stirring rod.
After all the H2SO4 has been added, remove the reaction tube from the ice and allow it to warm to room temperature...
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